Analytical Sample Bundle Metadata

2006

Re-analysis of NB till samples (1H2), NBDNRE, <63 micron size fraction – INAA + ICP-AES + ICP-MS  

Type: work order



Bundle Description

232 till samples from surveys across New Brunswick were re-analysed in 2006.  The samples were analysed in an attempt to “level” the analytical data from numerous surveys which had been analysed previously by a variety of methods in different laboratories.

The samples were analysed for 7 trace elements using inductively coupled plasma mass spectrometry (ICP-MS) and for 19 trace elements (including S, excluding Bi) using inductively coupled plasma atomic emission spectrometry (ICP-AES).  The samples were analysed for 33 trace elements (no Ca, Sr) using instrumental neutron activation analysis (INAA).  The analyses (1H2 package) were performed by Activation (Actlabs) Labs Ltd., Ancaster, Ontario.

Analytical Package Description

Laboratory: Activation Laboratories Limited, Ancaster, Ontario

Name: ActLabs (1H2) (v2) INAA + ICP-AES + ICP-MS ( more)

Analytical Suites:

Index Name
1  ActLabs ICP-MS (7 elements; Tl:0.1)
2  ActLabs INAA (33 elements; no Ca, Sr)
3  ActLabs ICP-AES (19 elements; 4-acid; inc S, ex Bi)

Analytical Methods:

Index Column Name Suite Order Method Order Suite Repeat Quantity Units Determination Limit
1  Bi_ICPMS    Bi   ppm 0.1  
2  Ge_ICPMS    Ge   ppm 0.1  
3  In_ICPMS    In   ppm 0.2  
4  Se_ICPMS    Se   ppm 0.1  
5  Sn_ICPMS    Sn   ppm 1  
6  Te_ICPMS    Te   ppm 0.1  
7  Tl_ICPMS    Tl   ppm 0.1  
8  Ag_INA    Ag   ppm 5  
9  As_INA    As   ppm 0.5  
10  Au_INA    Au   ppb 2  
11  Ba_INA    Ba   ppm 50  
12  Br_INA    Br   ppm 0.5  
13  Ce_INA    Ce   ppm 3  
14  Co_INA    Co   ppm 1  
15  Cr_INA    Cr   ppm 2  
16  Cs_INA    Cs   ppm 1  
17  Eu_INA  10    Eu   ppm 0.2  
18  Fe_INA  11    Fe   percent 0.01  
19  Hf_INA  12    Hf   ppm 1  
20  Hg_INA  13    Hg   ppm 1  
21  Ir_INA  14    Ir   ppb 5  
22  La_INA  15    La   ppm 0.5  
23  Lu_INA  16    Lu   ppm 0.05  
24  Mo_INA  17    Mo   ppm 1  
25  Na_INA  18    Na   percent 0.01  
26  Nd_INA  19    Nd   ppm 5  
27  Ni_INA  20    Ni   ppm 20  
28  Rb_INA  21    Rb   ppm 15  
29  Sb_INA  22    Sb   ppm 0.1  
30  Sc_INA  23    Sc   ppm 0.1  
31  Se_INA  24    Se   ppm 3  
32  Sm_INA  25    Sm   ppm 0.1  
33  Sn_INA  26    Sn   ppm 100  
34  Ta_INA  27    Ta   ppm 0.5  
35  Tb_INA  28    Tb   ppm 0.5  
36  Th_INA  29    Th   ppm 0.2  
37  U_INA  30    U   ppm 0.5  
38  W_INA  31    W   ppm 1  
39  Yb_INA  32    Yb   ppm 0.2  
40  Zn_INA  33    Zn   ppm 50  
41  Wt_INA  34    Wt   grams  
42  Ag_ICPES    Ag   ppm 0.3  
43  Al_ICPES    Al   percent 0.01  
44  Be_ICPES    Be   ppm 1  
45  Ca_ICPES    Ca   percent 0.01  
46  Cd_ICPES    Cd   ppm 0.3  
47  Cu_ICPES    Cu   ppm 1  
48  K_ICPES    K   percent 0.01  
49  Mg_ICPES    Mg   percent 0.01  
50  Mn_ICPES    Mn   ppm 1  
51  Mo_ICPES  10    Mo   ppm 1  
52  Ni_ICPES  11    Ni   ppm 1  
53  P_ICPES  12    P   percent 0.001  
54  Pb_ICPES  13    Pb   ppm 3  
55  S_ICPES  14    S   percent 0.01  
56  Sr_ICPES  15    Sr   ppm 1  
57  Ti_ICPES  16    Ti   percent 0.01  
58  V_ICPES  17    V   ppm 2  
59  Y_ICPES  18    Y   ppm 1  
60  Zn_ICPES  19    Zn   ppm 1  
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