Analytical Suite Metadata

GSC: uranium by fluorometry



General Methodology:

U by fluorometry

400 mg of minus 250 mesh sediment are weighed out.  To this are added 6 ml of 4N HNO3 and 2 drops of concentrated HCl.  The sample is shaken and placed in a water bath at 90°C for 1.5 hours.  The sample is then diluted to 20 ml with metal-free water, with intermittent agitation and allowed to settle.  A 0.2 mlaliquot of the leach is placed on a Pt dish and evaporated to dryness.  The residue is burned for 1 minute above a Bunsen flame.  To this are added 3g of a K2CO3-Na2CO3-NaF flux.  The sample is then fused for 10 minutes at 650°C, cooled in a dessicator, and the U concentration read on a Jarrel-Ash fluorometer.

Instrument:

Sample material: solid

Sample weight: 400 milligrams


Analytical Technique:

Hierarchical classification

Technique >> Photometry >> Fluorometry

Children

None


Analytical Decomposition:

Hierarchical classification

Decomposition >> Aqueous dissolution >> Acid >> Moderate Acid >> Aqua Regia (s.l.)

Children

Aqua Regia (s.s.) | Lefort | Aqua Regia (Acme/BVM) | Aqua regia (NGR) | Aqua regia (NASGLP)


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  5998     U_Fluor  0.2

Associated Analytical Packages:

IndexPackage IDPackage Name
1  344     GSC Resource Geochemistry lake sediment analysis, Bear-Slave Operation
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