Analytical Suite Metadata

GSC cold vapour atomic absorption spectroscopy: Hg



General Methodology:

Hg in sediment

500 mg of less than 250 mesh material was leached with 20 ml conc. HNO3, 1 ml conc. HCl, and 80 ml H2O, at 95°C for 1.5 hours in a water bath.  The sample was cooled and a 100 ml aliquot was taken.  The solution was analysed using a Techtron AA-5 atomic absorption spectrophotometer, by a cold vapour method.  100 ml of 2.5% SnSO4 were added to the 100 ml aliquot.  The sample was aerated and the metallic Hg vapour released was determined at 253.7 nm.

Instrument:

Sample material: solid

Sample weight: 500 milligrams


Analytical Technique:

Hierarchical classification

Technique >> Spectroscopy >> Electromagnetic radiation >> Visible-ultraviolet >> Atomic >> Absorption >> Cold vapour

Children

None


Analytical Decomposition:

Hierarchical classification

Decomposition >> Aqueous dissolution >> Acid >> Moderate Acid >> Aqua Regia (s.l.)

Children

Aqua Regia (s.s.) | Lefort | Aqua Regia (Acme/BVM) | Aqua regia (NGR) | Aqua regia (NASGLP)


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  5997     Hg_CVAAS  2

Associated Analytical Packages:

IndexPackage IDPackage Name
1  344     GSC Resource Geochemistry lake sediment analysis, Bear-Slave Operation
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