Analytical Suite Metadata

Bondar Clegg (lake and stream sediment) AAS (Mo, V; nitrous oxide-acetylene)-reacted overnight at room temperature



Bondar Clegg, lake and stream sediment; atomic absorption spectroscopy (molybdenum, vanadium; nitrous oxide-acetylene)-reacted overnight at room temperature.

General Methodology:

Determination was by atomic absorption spectroscopy using a nitrous oxide acetylene flame.  A 0.5g sample is reacted with 1.5 ml concentrated HNO3 in a test tube overnight at room temperature.  After digestion, the test tube is immersed in a hot water bath at room temperature and brought up to 90oC and held at this temperature for 30 minutes with periodic shaking.  At this point, 0.5 ml concentrated HCl is added and the digestion continued at 90oC for an additional 90 minutes.  After cooling, 8 ml of 1250 ppm Al solution are added and the sample solution diluted to 10 ml before aspiration.

Instrument: unstated

Sample material: solid

Sample weight: 500 milligrams


Analytical Technique:

Hierarchical classification

Technique >> Spectroscopy >> Electromagnetic radiation >> Visible-ultraviolet >> Atomic >> Absorption >> Flame >> C2H2/N2O

Children

None


Analytical Decomposition:

Hierarchical classification

Decomposition >> Aqueous dissolution >> Acid >> Moderate Acid >> Aqua Regia (s.l.)

Children

Aqua Regia (s.s.) | Lefort | Aqua Regia (Acme/BVM) | Aqua regia (NGR) | Aqua regia (NASGLP)


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  1278     V_AAS  5
2  1279     Mo_AAS  2

Associated Analytical Packages:

IndexPackage IDPackage Name
1  467     Bondar Clegg (NGR lake sediment) AAS(8+3), CV(Hg), LOI, F
2  468     Bondar Clegg (NGR stream sediment, NV, 1995) AAS(8+4), CV(Hg), LOI, F
3  469     Bondar Clegg (NGR lake sediment) AAS(8+Cd,Mo,V), CV(Hg - d.l. 5ppb), LOI, F
4  470     Bondar Clegg (NGR stream sediment) AAS(8+4), CV(Hg – d.l. 5ppb), LOI, F
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