Analytical Suite Metadata

Bondar Clegg (lake sediment) Mo + V (2.5ml conc)

Bondar Clegg, lake sediment; Molybdenum + Vanadium (2.5ml concentrate)

General Methodology:

Determination was by atomic absorption spectroscopy using a nitrous oxide acetylene flame.  A 0.5 gram sample was reacted with 2.5 ml concentrated HNO3 at 90oC for 30 minutes.  At this point 0.5 ml concentrated HCl was added and the digestion was continued at 90oC for an additional 90 minutes.  After cooling, 8 ml of 1250 ppm Al solution were added and the sample solution was diluted to 10 ml before aspiration.

Instrument: unstated

Sample material: solid

Sample weight: 500 milligrams

Analytical Technique:

Hierarchical classification

Technique >> Spectroscopy >> Electromagnetic radiation >> Visible-ultraviolet >> Atomic >> Absorption >> Flame >> C2H2/N2O



Analytical Decomposition:

Hierarchical classification

Decomposition >> Aqueous dissolution >> Acid >> Moderate Acid >> Aqua Regia (s.l.)


Aqua Regia (s.s.) | Lefort | Aqua Regia (Acme/BVM) | Aqua regia (NGR) | Aqua regia (NASGLP)

Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  2236     Mo_AAS  2
2  2237     V_AAS  5

Associated Analytical Packages:

IndexPackage IDPackage Name
1  435     Bondar Clegg (NGR lake sediment) AAS(8+7), CV(Hg), LOI, W, F,
2  440     Bondar Clegg (NGR lake sediment) AAS (8+3+(Mo+V: 2.5 ml conc)), CVAAS (Hg), LOI, F, U(10**12)
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