Analytical Sample Bundle Metadata

1999

Atholville and Charlo, NB humus samples (Dickson, NBDNRE), 177 micron size fraction – AAS + Hg-CVAAS + LOI

Type: lab data



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Bundle Description

Geochemical results of humus samples collected in the Atholville (21O/15) and Charlo (21O/16) regions, north central New Brunswick.

The < 177 micron fraction of the humus samples was analysed for 12 trace elements using atomic absorption spectroscopy (AAS).  For determination of Ag, Cd, Co, Cu, Fe, Mn, Ni, Pb and Zn, atomic absorption spectroscopy (AAS) was performed with an air acetylene flame.  Determination of Mo and V was done by atomic absorption spectroscopy (AAS) using a nitrous oxide acetylene flame.  Mercury was determined by cold vapour atomic absorption spectrometry (Hg-CVAAS) using a modified Hatch and Ott procedure.  Loss on ignition (LOI) was also determined for the humus samples.  The analyses were carried out by CANTECH Laboratories in Calgary, Alberta.

Sample Classification (Analytical)

Index Sample Count Survey Sample Type Prep Lab Material Control Ref Unknown Source Duplicates count
1  109  Till sampling survey, NTS 21O/15 (Atholville), 21O/16 (Charlo), north central New Brunswick, 1998-1999. ( more)   Humus  <177 micron (NGR) No  No  0 

Analytical Package Description

Laboratory: CANTECH Laboratories, Calgary, Alberta

Name: CanTech AAS + Hg-CVAAS + LOI ( more)

…

Analytical Suites:

Index Name
1  CanTech AAS (unknown acid digestion)
2  CanTech AAS (Mo, V) (unknown acid digestion)
3  CanTech Hg-CVAAS (unknown acid digestion)
4  CanTech LOI

Analytical Methods:

Index Column Name Suite Order Method Order Suite Repeat Quantity Units Determination Limit
1  Ag_AAS  1  1  0    Ag   ppm 0.2  
2  Cd_AAS  1  2  0    Cd   ppm 0.2  
3  Co_AAS  1  3  0    Co   ppm  
4  Cu_AAS  1  4  0    Cu   ppm  
5  Fe_AAS  1  5  0    Fe   percent  
6  Mn_AAS  1  6  0    Mn   ppm  
7  Ni_AAS  1  7  0    Ni   ppm  
8  Pb_AAS  1  8  0    Pb   ppm  
9  Zn_AAS  1  9  0    Zn   ppm  
10  Mo_AAS  2  1  0    Mo   ppm 1  
11  V_AAS  2  2  0    V   ppm  
12  Hg_AAS  3  1  0    Hg   ppb  
13  LOI  4  1  0    LOI   percent  
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