Analytical Suite Metadata

ACME (stream sediment) ICP-MS (Sn - LiBO2 fusion)



ACME, stream sediment, ICP-MS (Sn - LiBO2 fusion)

General Methodology:

Tin was analysed by heating a 0.2g sample mixed with 1.5g of LiBO2 flux in a muffle furnace for 15 minutes at 1050°C in a graphite crucible. The molten mixture was removed and immediately poured into 100ml of 5% HNO3.  The solution was shaken for two hours and then an aliquot was poured into a test tube.  Analytical values were determined using a Perkin-Elmer 6000 ICP-MS.

Instrument:

Sample material: solid

Sample weight: unstated


Analytical Technique:

Hierarchical classification

Technique >> Spectroscopy >> Mass >> ICP-MS

Children

None


Analytical Decomposition:

Hierarchical classification

Decomposition >> Fusion

Children

Acidic (fusion) | Alkaline | Ammonium halide | Combustion | Fire Assay


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  2445     Sn  1

Associated Analytical Packages:

IndexPackage IDPackage Name
1  489     Acme (NGR stream sediment) IPC-MS / ICP-ES (35 element), LOI, Sn (LiBO2 fusion), F
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