Analytical Suite Metadata

ACME (stream  sediment) ICP-MS / ICP-ES (35 elements, W, d.l. = 0.2ppm)



ACME, stream  sediment; ICP-MS / ICP-ES (Ag, Al, As, Ba, Bi, Cd, Ca, Co, Cr, Cu, Fe, Ga, Hg, K, La, Mg, Mn, Mo, Na, Ni, P, Pb, S, Sb, Sc, Se, Sr, Te, Th, Ti, Tl, U, V, W (d.l.=0.2 ppm), Zn)

General Methodology:

A one gram sample is leached with 6ml of a mixture of HCl, HNO3, and distilled, deionized water (2:2:2 v/v) at 95°C for one hour.  The sample solution is diluted to 20ml and analysed by inductively coupled plasma emission spectroscopy on a Jarrell Ash instrument and inductively couple plasma mass spectroscopy on a Perkin Elmer Elan instrument.

Instrument:

Sample material: solid

Sample weight: unstated


Analytical Technique:

Hierarchical classification

Technique >> Other >> ICP-MS/ICP-ES

Children

None


Analytical Decomposition:

Hierarchical classification

Decomposition >> Aqueous dissolution >> Acid >> Moderate Acid >> Aqua Regia (s.l.) >> Aqua Regia (Acme/BVM) >> Aqua Regia (Acme)

Children

None


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  2288     Ag_ICPMS_ES  2
2  2289     Al_ICPMS_ES  0.01
3  2290     As_ICPMS_ES  0.1
4  2291     Ba_ICPMS_ES  0.5
5  2292     Bi_ICPMS_ES  0.02
6  2293     Cd_ICPMS_ES  0.01
7  2294     Ca_ICPMS_ES  0.01
8  2295     Co_ICPMS_ES  0.1
9  2296     Cr_ICPMS_ES  0.5
10  10  2297     Cu_ICPMS_ES  0.01
11  11  2298     Fe_ICPMS_ES  0.01
12  12  2299     Ga_ICPMS_ES  0.1
13  13  2300     Hg_ICPMS_ES  5
14  14  2301     K_ICPMS_ES  0.01
15  15  2302     La_ICPMS_ES  0.5
16  16  2303     Mg_ICPMS_ES  0.01
17  17  2304     Mn_ICPMS_ES  1
18  18  2305     Mo_ICPMS_ES  0.01
19  19  2306     Na_ICPMS_ES  0.001
20  20  2307     Ni_ICPMS_ES  0.1
21  21  2308     P_ICPMS_ES  0.001
22  22  2309     Pb_ICPMS_ES  0.01
23  23  2310     S_ICPMS_ES  0.01
24  24  2311     Sb_ICPMS_ES  0.02
25  25  2312     Sc_ICPMS_ES  0.1
26  26  2313     Se_ICPMS_ES  0.1
27  27  2314     Sr_ICPMS_ES  0.5
28  28  2315     Te_ICPMS_ES  0.02
29  29  2316     Th_ICPMS_ES  0.1
30  30  2317     Ti_ICPMS_ES  0.001
31  31  2318     Tl_ICPMS_ES  0.02
32  32  2319     U_ICPMS_ES  0.1
33  33  2320     V_ICPMS_ES  2
34  34  2321     W_ICPMS_ES  0.2
35  35  2322     Zn_ICPMS_ES  0.1

Associated Analytical Packages:

IndexPackage IDPackage Name
1  463     Acme (NGR stream sediment) IPC-MS / ICP-ES (35 elements, W, d.l.=0.2 ppm ), Sn, LOI
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