Analytical Suite Metadata

Bondar Clegg (lake sediment) AAS (8 + Cd; air acetylene) 6ml decomp: 4HNO3 1HCL



Bondar Clegg, lake sediment; atomic absorption spectroscopy  (8 elements: Zn, Cu, Pb, Ni, Co, Ag, Mn, Fe + Cd; air acetylene) 6ml decomp: 4HNO3 1HCL

General Methodology:

A 1 gram sample was reacted with 6 ml of a mixture of 4 M HNO3 and M HCl in a test-tube overnight at room temperature.  After digestion, the test-tube was immersed in a hot water bath at room temperature and brought up to 90oC and held at this temperature for two hours with periodic shaking.  The sample solution was then diluted to 20 ml with metal free water and mixed.  The element was determined by atomic absorption spectroscopy using an air-acetylene flame.

Background corrections were made for Pb, Ni, Co, Ag and Cd.

Instrument: unstated

Sample material: solid

Sample weight: unstated


Analytical Technique:

Hierarchical classification

Technique >> Spectroscopy >> Electromagnetic radiation >> Visible-ultraviolet >> Atomic >> Absorption >> Flame >> C2H2/Air

Children

None


Analytical Decomposition:

Hierarchical classification

Decomposition >> Aqueous dissolution >> Acid >> Moderate Acid >> Aqua Regia (s.l.) >> Aqua regia (NGR)

Children

Aqua regia (NGR-S) | Aqua regia (NGR-L) | Aqua regia (NGR-S, no details) | Aqua regia (NGR-L, no details) | Aqua regia (NGR-LS) | Aqua regia (NGR-S, alternate) | Aqua regia (NGR-L, alternate) | Aqua regia (NGR-S, BC)


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  2181     Zn_AAS  2
2  2182     Cu_AAS  2
3  2183     Pb_AAS  2
4  2184     Ni_AAS  2
5  2185     Co_AAS  2
6  2186     Ag_AAS  0.2
7  2187     Mn_AAS  5
8  2188     Fe_AAS  0.02
9  2189     Cd_AAS  0.2

Associated Analytical Packages:

IndexPackage IDPackage Name
1  419     Bondar Clegg (NGR lake sediment) AAS (8+5), CVAAS (Hg), LOI, F, U(5**10, He detector, 20s, d.l.=0.5)
2  421     Bondar Clegg (NGR lake sediment) AAS 8+6+Ba (HCLO4 only)), CVAAS (Hg),W, LOI, F, U(10**12)
3  423     Bondar Clegg (NGR lake sediment) AAS (8+5), CVAAS (Hg), LOI, F, U(10**12)
4  429     Bondar Clegg (NGR lake sediment) AAS (8+5), CV(Hg), LOI at 500C, F, U - 10**12 flux
5  432     Bondar Clegg (NGR lake sediment) AAS(8+7), CV(Hg), LOI, W, F, U
6  435     Bondar Clegg (NGR lake sediment) AAS(8+7), CV(Hg), LOI, W, F,
7  440     Bondar Clegg (NGR lake sediment) AAS (8+3+(Mo+V: 2.5 ml conc)), CVAAS (Hg), LOI, F, U(10**12)
8  466     Bondar Clegg (NGR lake sediment) AAS(8+3), CV(Hg - d.l. 5ppb), LOI, F
9  467     Bondar Clegg (NGR lake sediment) AAS(8+3), CV(Hg), LOI, F
10  469     Bondar Clegg (NGR lake sediment) AAS(8+Cd,Mo,V), CV(Hg - d.l. 5ppb), LOI, F
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