Analytical Suite Metadata

Barringer (surface water) ISE (F) (NGR, BC, 1986)



Barringer, surface water; ion-selective electrode (fluorine)

General Methodology:

Fluoride in water samples was determined using a fluoride electrode.  Prior to measurement an aliquot of the sample was mixed with an equal volume of TISAB II buffer solution (total ionic strength adjustment buffer).  The TISAB II buffer solution is prepared as follows: to 50 ml metal free water add 57 ml glacial acetic acid, 58 gm NaCl and 4 gm CDTA (cyclohexylene dinitrilo tetraacetic acid).  Stir to dissolve and cool to room temperature.  Using a pH meter, adjust the pH between 5.0 and 5.5 by slowly adding 5 M NaOH solution. Cool and dilute to one litre in a volumetric flask.

Instrument: unstated

Sample material: aqueous

Sample weight: unstated


Analytical Technique:

Hierarchical classification

Technique >> Electrochemical techniques >> Potentiometry >> Ion-specific electrodes

Children

Glass electrode


Analytical Decomposition:

Hierarchical classification

Decomposition >> None

Children

None


Analytical Methods:

IndexMethod OrderMethod IDQuantityDetection Limit
1  1021     F_ISE  20

Associated Analytical Packages:

IndexPackage IDPackage Name
1  418     Bondar Clegg (NGR surface water) LIF(U), ISE(F), pH
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